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KMID : 1059520130570050547
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Journal of the Korean Chemical Society
2013 Volume.57 No. 5 p.547 ~ p.553
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Fabrication and Characterization Nano Porous Anodic ZrO2 Membranes by Two-Step Anodizing
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Seo Eui-Young
Choi Se-Kyeong
Shin Ik-Soo
Kang Wee-Kyung
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Abstract
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Zirconium oxide (ZrO2) nano porous membranes were fabricated by electrochemical two-step anodization with an electropolished zirconium substrate in inorganic water-based and organic electrolyte systems containing small amounts of fluoride. Using two-step anodization and organic electrolytes, highly regular and ordered nanotubular ZrO2 oxide layers can be compared with aqueous electrolytes. The morphology and size of the nano porous layers were characterized by FE-SEM (field emission scanning electron microscopy), XRD (X-ray diffraction), and EDS (energy dispersive spectroscopy). Luminescence properties were investigated by photoluminescence measurements.
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KEYWORD
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Electrochemistry, Nano-porous oxide film, Anodizing, ZrO2
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